Glassy Carbon Round Robin: Difference between revisions

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==Samples==
==Samples==
Two samples of glassy carbons from Jan Ilavsky have made their way (as of Dec 1 2008) to NIST, ILL and ISIS and will head on to Diamond and APS.
Two samples of glassy carbons (labeled C4 and G9) from Jan Ilavsky have made their way (as of Dec 1 2008) to NIST, ILL and ISIS and will head on to Diamond and APS. Additionally another sample, labeled G8, has been measured at ISIS.


The samples are:
The samples are cut from glassy carbon material, manufactured by Alpha Aesar under description: Glassy Carbon type 2. These samples are manufactured in 50 x 50 mm plates,  nominally 1 mm thick. Measurements with a micrometer were all between 0.99 and 1.01 mm.  The following reference describes the type of material that has been used for this round-robin and some X-ray scattering results:


Samples were cut from glassy carbon manufactured by Alpha Aesar under description: Glassy Carbon type 2. These samples are manufactured in 50 x 50 mm plates, 1 mm thick.
Fan Zhang, Jan Ilavsky, Gabrielle G. Long, John P.G. Quintana,
Andrew J. Allen, and Pete R. Jemian, “Glassy Carbon as an Absolute Intensity Calibration Standard for Small-Angle Scattering”, Metallurgical and Materials Transactions A  DOI: 10.1007/s11661-009-9950-x


===C4===
==Data Format==


===G9===
Contributors are encouraged to deposit their data using the
[[cansas1d_documentation | cansas1d/1.0 XML data standard for 1-D SAS data]] within a ZIP or gzip archive file. 
A WWW form ([http://www.smallangles.net/canSAS/xmlWriter/ canSAS/xmlWriter])
is available to translate three-column ASCII text data into the
canSAS1d/1.0 XML format.


Include the default XSLT stylesheet ([http://svn.smallangles.net/svn/canSAS/1dwg/trunk/cansasxml-html.xsl cansasxml-html.xsl]) in the archive and make sure that each XML file has a reference to that stylesheet in the file header:
<pre>
<?xml version="1.0"?>
<?xml-stylesheet type="text/xsl" href="cansasxml-html.xsl" ?>
<SASroot ...
</pre>
==Data Repository==
All the data on this page is available in a subversion repository:
<pre>
svn co http://svn.smallangles.net/svn/canSAS/1dwg/data
</pre>


==Experimental details and Data==
==Experimental details and Data==
Line 15: Line 33:
===NIST===
===NIST===


<Gallery caption="NIST data for C4 and G9" widths="300px" heights="200px">
Image:C4.jpg|C4
Image:G9.jpg|G9
</Gallery>
Zip file of all data (in NIST 6 column format) with plots in PDF and Igor Pro formats [[Media:GlassyCarbon_NIST.zip|GlassyCarbon_NIST.zip]]
Zip file of all data (in canSAS XML 1D format) [[Media:GlassyCarbon_NIST_XML.zip|GlassyCarbon_NIST_XML.zip]]


===ILL===
===ILL===


====2009 Data====
<Gallery caption="ILL data for C4 and G9" widths="300px" heights="200px">
Image:ILL_Comparison_Aug09.jpg|Comparison plot
</Gallery>
Zip file of all data (in ILL reduced ascii and canSAS XML) with comparison plot JPEG [[Media:GlassyCarbon_ILL_Aug09.zip|GlassyCarbon_ILL_Aug09.zip]]
====2008 Data====
<Gallery caption="ILL data for C4 and G9" widths="100px" heights="50px">
Image:C4_zoom.jpg|C4
Image:G9_zoom.jpg|G9
</Gallery>
* Data from 2008 should be ignored.  Apparently there was an error in the reduction.
Zip file of 2008 data (in NIST 6 column format) with plots in PDF and Igor Pro formats [[Media:GlassyCarbon_ILL.zip|GlassyCarbon_ILL.zip]]
Zip file of 2008 data (in canSAS XML 1D format) [[Media:GlassyCarbon_ILL_XML.zip|GlassyCarbon_ILL_XML.zip]]


===ISIS===
===ISIS===


The collected data in canSAS XML format : [[Media:GLASSYC_C4G8G9.XML‎|GLASSYC_C4G8G9.XML‎]]
<Gallery caption="ISIS data for C4 and G9" widths="300px" heights="200px">
Image:LOQ_C4.jpg|C4
Image:LOQ_G9.jpg|G9
</Gallery>
 
The collected data in canSAS XML format : [[Media:GLASSYC_C4G8G9.XML‎|GLASSYC_C4G8G9.XML‎]] and in pseudo canSAS XML (includes T vs Lambda datasets): [[Media:GLASSYC_C4G8G9_withTL.XML‎|GLASSYC_C4G8G9_withTL.XML‎]]
 
Zip archive file with above XML files and standard stylesheet: [[Media:GLASSYC_C4G8G9.zip‎|GLASSYC_C4G8G9.zip]]


Excel file of that data with plots : [[Media:Glassy_Carbons_C4_G8_G9.xls‎|Glassy_Carbons_C4_G8_G9.xls‎]]
Excel file of that data with plots : [[Media:Glassy_Carbons_C4_G8_G9.xls‎|Glassy_Carbons_C4_G8_G9.xls‎]]
===APS USAXS===
<Gallery caption="APS data for C4 and G9" widths="300px" heights="200px">
Image:C4_APS.jpg|C4
Image:G9_APS.jpg|G9
</Gallery>
Zip file of all data (in ASCII 3 column format) with plots in PDF and Igor Pro formats [[Media:GlassyCarbon_APS.zip|GlassyCarbon_APS.zip]]
Zip file of all data (in canSAS XML 1D format) [[Media:GlassyCarbon_APS_XML.zip|GlassyCarbon_APS_XML.zip]]
===ESRF ID01 PINHOLE===
The calibration sample measured on ID01 is designated "Glassy Carbon type 2 C, sample C14", thickness 1 mm.
The scattering intensity has been determined by cross calibration with a secondary standard ("lupolen BL4"). The
scattering intensity of this sample decreases locally with the absorbed dose where irradiated. The unirradiated parts of
this sample have identical scattering intensities that are higher than the scattering intensites of the irradiated parts.
The calibration factor was found by scanning the secondary standard and using only an unirradiated part for calibration.
Due to the uncertainties of the sample the accuracy of the absolute calibration is not assumed to be better than +-20%.
The error bars indicate the statistical errors that are practically neglegible (typically 0.1% of the data values).
<Gallery caption="ESRF ID01 PINHOLE data for C14" widths="300px" heights="200px">
Image:C14 ESRF ID01 PINHOLE.PNG
</Gallery>
Zip file of all data (in ASCII 3 column format) [[Media:GlassyCarbon_ESRF_ID01.zip|GlassyCarbon_ESRF_ID01.zip]]
===ESRF ID02 USAXS===
The calibration sample measured on ID02 is designated "Glassy Carbon type 2 C, sample C14", thickness 1 mm.
The scattering intensity has been calibrated with the USAXS camera relative to the primary beam without any cross calibration.
Remark: To increase the resolution at very low q-values a third crystal is mounted perpendicular to the scanning crystals.
This reduces the sensitivity at higher q-values. Therefore only the range from qmin=0.0002*nm to qmax=0.06*nm has been measured.
<Gallery caption="ESRF ID02 USAXS data for C14" widths="300px" heights="200px">
Image:C14 ESRF ID02 USAXS.PNG
</Gallery>
Zip file of all data (in ASCII 3 column format) [[Media:GlassyCarbon_ESRF_ID02.zip|GlassyCarbon_ESRF_ID02.zip]]
=== Diamond I22 ===
<Gallery caption="DLS I22 SAXS data for C14" widths="300px" heights="200px">
Image:gc14-i22-dls.jpg
</Gallery>
SAXS data, 8.9 keV, in canSAS XML format [[Media:gc14-dls-i22.xml‎|gc14-dls-i22.xml‎]] and ZIP archive [[Media:gc14-dls-i22.zip|gc14-dls-i22.zip]].

Latest revision as of 10:59, 20 September 2009

Samples

Two samples of glassy carbons (labeled C4 and G9) from Jan Ilavsky have made their way (as of Dec 1 2008) to NIST, ILL and ISIS and will head on to Diamond and APS. Additionally another sample, labeled G8, has been measured at ISIS.

The samples are cut from glassy carbon material, manufactured by Alpha Aesar under description: Glassy Carbon type 2. These samples are manufactured in 50 x 50 mm plates, nominally 1 mm thick. Measurements with a micrometer were all between 0.99 and 1.01 mm. The following reference describes the type of material that has been used for this round-robin and some X-ray scattering results:

Fan Zhang, Jan Ilavsky, Gabrielle G. Long, John P.G. Quintana, Andrew J. Allen, and Pete R. Jemian, “Glassy Carbon as an Absolute Intensity Calibration Standard for Small-Angle Scattering”, Metallurgical and Materials Transactions A DOI: 10.1007/s11661-009-9950-x

Data Format

Contributors are encouraged to deposit their data using the cansas1d/1.0 XML data standard for 1-D SAS data within a ZIP or gzip archive file. A WWW form (canSAS/xmlWriter) is available to translate three-column ASCII text data into the canSAS1d/1.0 XML format.

Include the default XSLT stylesheet (cansasxml-html.xsl) in the archive and make sure that each XML file has a reference to that stylesheet in the file header: 

<?xml version="1.0"?>
<?xml-stylesheet type="text/xsl" href="cansasxml-html.xsl" ?>
 <SASroot ...

Data Repository

All the data on this page is available in a subversion repository: 

svn co http://svn.smallangles.net/svn/canSAS/1dwg/data

Experimental details and Data

NIST

  • NIST data for C4 and G9
  • C4

    C4

  • G9

    G9


Zip file of all data (in NIST 6 column format) with plots in PDF and Igor Pro formats GlassyCarbon_NIST.zip

Zip file of all data (in canSAS XML 1D format) GlassyCarbon_NIST_XML.zip

ILL

2009 Data

  • ILL data for C4 and G9
  • Comparison plot

    Comparison plot

Zip file of all data (in ILL reduced ascii and canSAS XML) with comparison plot JPEG GlassyCarbon_ILL_Aug09.zip


2008 Data

  • ILL data for C4 and G9
  • C4

    C4

  • G9

    G9

  • Data from 2008 should be ignored. Apparently there was an error in the reduction.

Zip file of 2008 data (in NIST 6 column format) with plots in PDF and Igor Pro formats GlassyCarbon_ILL.zip

Zip file of 2008 data (in canSAS XML 1D format) GlassyCarbon_ILL_XML.zip

ISIS

  • ISIS data for C4 and G9
  • C4

    C4

  • G9

    G9

The collected data in canSAS XML format : GLASSYC_C4G8G9.XML‎ and in pseudo canSAS XML (includes T vs Lambda datasets): GLASSYC_C4G8G9_withTL.XML‎

Zip archive file with above XML files and standard stylesheet: GLASSYC_C4G8G9.zip

Excel file of that data with plots : Glassy_Carbons_C4_G8_G9.xls‎

APS USAXS

  • APS data for C4 and G9
  • C4

    C4

  • G9

    G9


Zip file of all data (in ASCII 3 column format) with plots in PDF and Igor Pro formats GlassyCarbon_APS.zip

Zip file of all data (in canSAS XML 1D format) GlassyCarbon_APS_XML.zip

ESRF ID01 PINHOLE

The calibration sample measured on ID01 is designated "Glassy Carbon type 2 C, sample C14", thickness 1 mm.

The scattering intensity has been determined by cross calibration with a secondary standard ("lupolen BL4"). The scattering intensity of this sample decreases locally with the absorbed dose where irradiated. The unirradiated parts of this sample have identical scattering intensities that are higher than the scattering intensites of the irradiated parts. The calibration factor was found by scanning the secondary standard and using only an unirradiated part for calibration. Due to the uncertainties of the sample the accuracy of the absolute calibration is not assumed to be better than +-20%. The error bars indicate the statistical errors that are practically neglegible (typically 0.1% of the data values).

  • ESRF ID01 PINHOLE data for C14
  • C14 ESRF ID01 PINHOLE.PNG

Zip file of all data (in ASCII 3 column format) GlassyCarbon_ESRF_ID01.zip

ESRF ID02 USAXS

The calibration sample measured on ID02 is designated "Glassy Carbon type 2 C, sample C14", thickness 1 mm. The scattering intensity has been calibrated with the USAXS camera relative to the primary beam without any cross calibration.

Remark: To increase the resolution at very low q-values a third crystal is mounted perpendicular to the scanning crystals. This reduces the sensitivity at higher q-values. Therefore only the range from qmin=0.0002*nm to qmax=0.06*nm has been measured.

  • ESRF ID02 USAXS data for C14
  • C14 ESRF ID02 USAXS.PNG

Zip file of all data (in ASCII 3 column format) GlassyCarbon_ESRF_ID02.zip

Diamond I22

  • DLS I22 SAXS data for C14
  • gc14-i22-dls.jpg

SAXS data, 8.9 keV, in canSAS XML format gc14-dls-i22.xml‎ and ZIP archive gc14-dls-i22.zip.

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